Ivica Dacic met Kosovo's Hashim Thaci at talks chaired by EU foreign affairs chief Catherine Ashton.
BBC: Leaders of Serbia and Kosovo meet for first time
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"Despite all these long meetings, we do not have an agreement at this moment, " Mr Dacic told Serbian media.
BBC: Serbia-Kosovo talks fail to reach accord in Brussels
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Serbian Prime Minister Ivica Dacic stressed Belgrade would never recognise Kosovo's independence "supervised or unsupervised", and dismissed the decision as meaningless.