The effects of catalyst amount, reaction time, molar ratio of sec-butanol and acetic acid, and amount of deaquation reagent on the reaction were studied.
考查了催化剂用量、反应时间、醇酸物质的量比及带水剂用量对乙酸酯化率的影响。
2
The deaquation, melting, decomposing apex temperatures and water content of ciprofloxacin hydrochloride monohydrate crystals were measured by DSC and TG techniques respectively.