An improved method of synthesizing trimethyl orthoformate through azeotropic distillation by taking sodium methoxide in methanol and chloroform as raw materials has been presented by the author.
介绍了以甲醇钠甲醇溶液与氯仿为原料，采用共沸蒸馏法制备原甲酸三甲酯的改进工艺。
2
The nanosized TiO2 powder prepared by foam flotation method was compared with the sample prepared by azeotropic distillation method.
对泡沫悬浮法和共沸蒸馏法的防团聚效果进行了系统比较。
3
Impurities in the dioxane were determined. The analysis method has important directive value for separating and purifying 1, 4-dioxane with azeotropic rectification.