By solvent extraction, column chromatography, and crystallization, fexofenadine (96.3% purity) was obtained with yield 63.5%.
通过对发酵液进行溶媒抽提、柱层析、重结晶,得到纯品,收率达到63.5%,纯度96.3%。
2
After column chromatographic separation, re-crystallization treatment and supercritical fluid precipitation treatment, the purity of lutein is improved.
粗提物经柱层析分离,重结晶,再经过超临界流体沉淀处理后,可提高叶黄素的纯度。
3
Conclusion: Silica gel column chromatography and crystallization are simple and rapid methods to isolate gardenoside.