Ketones and stabilized phosphorus ylides were heated together in commercial microwave oven, under solvent and medium free conditions, the Wittig reaction finished within 4.
酮与稳定膦叶立德在家用微波炉中加热,在无任何溶剂或固体介质条件下,4。
2
The reaction was not suitable conducted under solvent-free condition, water formed during the reaction was removed by azeotropic distillation with toluene throughout the reaction.