Methods The compounds were isolated by silica gel, ODS, and macroporous resin column chromatography and their structures were determined by means of spectral analysis.
方法利用正相、反相硅胶柱和大孔树脂柱色谱分离，并通过波谱技术进行结构鉴定。
2
Methods Silica gel superfine process was conducted by combining solvent extraction and separation with macroporous absorbent resin.
方法首先用溶剂萃取结合大孔吸附树脂分离，然后用硅胶柱精制提取。
3
Method: Isolation and purification of the trace constituents were carried out mainly by solvents extraction and macroporous adsorbing resin and silica gel column chromatography.