Acetylation between alcohol and benzoyl oxide was carried out using ZnBr_2 as a Lewisacidcatalyst in solvent-free condition. Some structures were characterized by NMR and IR.
以溴化锌为催化剂,在无溶剂条件下实现了醇与苯甲酸酐的酰化反应,部分产物经NMR和IR表征。
2
IR pattern indicated that Lewisacid centers mainly exist on the catalyst surface.
红外光谱测试结果表明,催化剂表面主要存在L酸中心。
3
The author used lewisacid as the catalyst and found the yield was raised as high as 67%.