The synthesis of lemonile perfume from litsea cubeba oil is newly studied and re-formed.
本文对利用山苍子油中柠檬醛合成柠檬腈香料进行了新探和改进。
2
Lemonile was manufactured by the dehydration of citral oxime obtained by the reaction of hydroxylamine sulfuride and citral abstracted from litsea cubeba oil.
从山苍子提取出的柠檬醛，与硫酸羟胺反应生成柠朦肟，脱水后可得到柠檬腈。
3
The catalytic dehydration of lemonile with various alkalis and PTC was studied. The optimal conditions dehydration to lemonile for KOH TBAB catalytic by orthogonal design were determined.