Based on it, the synthesis method has been improved. Several new compounds have been prepared by the Grignardreaction of its hydrogenation product.
在此基础上，改进了它的合成方法，并通过它的氢化产物的格氏反应，制备了一些新的化合物。
2
According to the mechanism of the exchange of metal-halogen, the time and temperature of reaction is proper extended, and the quality of reaction of grignard is improved.
根据金属—卤素交换的机理，适当的延长时间和降低温度，使格利雅合成的质量得到提高。
3
The synthesis methods of hexamethyldisilane, such as reductive coupling reaction, Grignard reagent alkylation, electrochemical reduction et al, were recounted in details.