METHODS:This compound was synthesize by steps of ammonolysis, hydrogenize, diazotization and coupling from 4 nitrobenzoyl chloride.
方法:以对硝基苯甲酰氯为原料,经氨解、氢化、重氮化及偶合四步反应得到了巴柳氮。
2
The reaction conditions for the synthesis were studied. The optimum parameters were given. The new technology for the hydrogenize reduction was researched.